Resumen
In the present work the effect of surface roughness on oxidation behavior during the early stages of high temperature exposure of Ni-base superalloy IN 625 is described. The surface roughness was described using standard contact profilometer as well as novel method, fractal analysis. It was found that the different surface preparation resulted in a difference in roughness with a parameter increase of at least one order of magnitude for the ground sample as compared with the polished sample. The oxidation test was performed in a horizontal tube furnace. Post-exposure analyses including glow discharge optical emission spectrometry (GD-OES) and scanning electron microscopy (SEM), which revealed that grinding lowers the oxidation kinetics of IN 625 from 1.76 × 10-12 cm2·s-1, obtained for polished sample, to 9.04 × 10-13 cm2·s-1. It was found that surface preparation influences the oxide scale composition and morphology. The hypothesis explaining the mechanism responsible for the changes in oxidation behavior is proposed as well.