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Inicio  /  Applied Sciences  /  Vol: 10 Par: 18 (2020)  /  Artículo
ARTÍCULO
TITULO

Experimental Study of Electrical Properties of Pharmaceutical Materials by Electrical Impedance Spectroscopy

Manuel Vázquez-Nambo    
José-Antonio Gutiérrez-Gnecchi    
Enrique Reyes-Archundia    
Wuqiang Yang    
Marco-A. Rodriguez-Frias    
Juan-Carlos Olivares-Rojas and Daniel Lorias-Espinoza    

Resumen

The physicochemical characterization of pharmaceutical materials is essential for drug discovery, development and evaluation, and for understanding and predicting their interaction with physiological systems. Amongst many measurement techniques for spectroscopic characterization of pharmaceutical materials, Electrical Impedance Spectroscopy (EIS) is powerful as it can be used to model the electrical properties of pure substances and compounds in correlation with specific chemical composition. In particular, the accurate measurement of specific properties of drugs is important for evaluating physiological interaction. The electrochemical modelling of compounds is usually carried out using spectral impedance data over a wide frequency range, to fit a predetermined model of an equivalent electrochemical cell. This paper presents experimental results by EIS analysis of four drug formulations (trimethoprim/sulfamethoxazole C14H18N4O3-C10H11N3O3, ambroxol C13H18Br2N2O.HCl, metamizole sodium C13H16N3NaO4S, and ranitidine C13H22N4O3S.HCl). A wide frequency range from 20 Hz to 30 MHz is used to evaluate system identification techniques using EIS data and to obtain process models. The results suggest that arrays of linear R-C models derived using system identification techniques in the frequency domain can be used to identify different compounds.

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